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Toribio et al 2019a - Revision history
2026-04-21T22:04:29Z
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Materiales.Compuestos at 15:53, 24 October 2022
2022-10-24T15:53:13Z
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<td colspan='2' style="background-color: white; color:black; text-align: center;">← Older revision</td>
<td colspan='2' style="background-color: white; color:black; text-align: center;">Revision as of 15:53, 24 October 2022</td>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">A.Toribio<sup>a</sup>, M.G. Prolongo<sup>a</sup>, C. Salom<sup>a</sup>, A.J. Martínez-Martínez<sup>a</sup>, S.G. Prolongo<sup>b</sup> </div></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;"><sup>a</sup>Dpto. Materiales y Producción Aeroespacial, E.T.S.I. Aeronáutica y del Espacio, Universidad Politécnica de Madrid </span></div></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;"><sup>b</sup>Dpto. Materiales y Producción Aeroespacial, E.T.S.I. Aeronáutica y del Espacio, Universidad Politécnica de Madrid, España</span></div></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">{| style="width: 87%;border-collapse: collapse;" </del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|-</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  colspan='2'  style="vertical-align: top;"|<big>Curado de nanocompuestos grafeno-epoxi: influencia de la  relación entrecruzante/resina</big></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|-</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  style="border-bottom: 1pt solid black;vertical-align: top;"|<span style="text-align: center; font-size: 75%;"> [[Image:Toribio_et_al_2019a-image1.png|54px]] </span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  style="vertical-align: top;"|</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|-</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  style="border-top: 1pt solid black;border-bottom: 1pt solid black;vertical-align: top;"|<span style="text-align: center; font-size: 75%;">Historia del artículo:</span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">Recibido 5 de Mayo 2017</span></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">En la versión revisada 5 de Mayo 2017</span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">Aceptado 31 de Mayo 2017</span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">Accesible online 21 de Junio 2017</span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  rowspan='4' style="vertical-align: top;"|<span style="text-align: center; font-size: 75%;">En el presente trabajo se estudia la influencia del tipo de grafeno (GNP) y las diferentes proporciones agente entrecruzante (XB) en el curado de dispersiones  grafeno-epoxi y en la temperatura de transición vítrea (''T<sub>g</sub>''</span><span style="text-align: center; font-size: 75%;">) del nanocomposite formado. La resina epoxi tipo DGEBA (LY) se ha entrecruzado con una poliamina aromática (XB). Se han utilizado dos tipos de grafeno: uno no funcionalizado (GNP<sub>n</sub></span><span style="text-align: center; font-size: 75%;">) y otro amino funcionalizado (GNP<sub>NH2</sub></span><span style="text-align: center; font-size: 75%;">.). En los dos sistemas se han estudiado 5 composiciones con diferente relación XB/LY y se ha variado el contenido de grafeno (6 y 10% en peso). La reacción de curado se ha estudiado por Calorimetría Diferencial de Barrido. Se ha observado que la presencia de grafeno acelera la reacción de curado y que la entalpía de reacción depende de la estequiometría y del contenido en grafeno. Se ha encontrado también que la variación de la ''T''</span><span style="text-align: center; font-size: 75%;">''<sub>g</sub>''</span><span style="text-align: center; font-size: 75%;"> del material con la estequiometria, depende del protocolo de curado. </span></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">.</span></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  style="border-top: 1pt solid black;vertical-align: top;"|<span style="text-align: center; font-size: 75%;">Palabras clave:</span></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|-</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  colspan='2'  style="vertical-align: top;"|<big>Curing of graphene-epoxy nanocomposites: influence of cross-linking / resin ratio </big></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  style="border-bottom: 1pt solid black;vertical-align: top;"|<span style="text-align: center; font-size: 75%;"> [[Image:Toribio_et_al_2019a-image2.png|54px]] </span></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">Graphene-epoxy</span></del></div></td><td colspan="2"> </td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"><span style="text-align: center; font-size: 75%;">Curing</span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  rowspan='2' style="vertical-align: top;"|<span style="text-align: center; font-size: 75%;">In the present work the influence of the graphene type (GNP) and the different crosslinking agent ratios in the curing of graphene-epoxy dispersions and in the glass transition temperature (''T<sub>g</sub>'') of the formed nanocomposite is studied. The epoxy resin type DGEBA (LY) has been crosslinked with an aromatic polyamine (XB). Two types of graphene have been used: one non-functionalized (GNP<sub>n</sub>) and another functionalized with amino groups  (GNP<sub>NH2</sub>). In the two systems, 5 compositions with different XB / LY ratios have been studied and, the content of graphene has been varied (6 and 10% by weight). The curing reaction has been studied by Differential Scanning Calorimetry. It has been observed that the presence of graphene accelerates the curing reaction and that the enthalpy of reaction depends on stoichiometry and graphene content. It has also been found that the variation of the ''T<sub>g</sub> ''of the material with the stoichiometry, depends on the curing protocol.</span></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|-</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|  style="border-top: 1pt solid black;vertical-align: top;"|</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;">|}</del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del style="font-weight: bold; text-decoration: none;"></del></div></td><td colspan="2"> </td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>==1 Introducción ==</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>==1 Introducción ==</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l93" >Line 93:</td>
<td colspan="2" class="diff-lineno">Line 32:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>En la Figura 2 se muestra la dependencia de la temperatura del pico exotérmico con la estequiometría para los distintos sistemas.</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>En la Figura 2 se muestra la dependencia de la temperatura del pico exotérmico con la estequiometría para los distintos sistemas.</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div> </div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>[[<ins class="diffchange diffchange-inline">File</ins>:Toribio_et_al_2019a-image6-c.png|<ins class="diffchange diffchange-inline">centre|600x600px</ins>]]</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>[[<del class="diffchange diffchange-inline">Image</del>:Toribio_et_al_2019a-image6-c.png|<del class="diffchange diffchange-inline">600px</del>]]</div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div></div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td></tr>
<tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l102" >Line 102:</td>
<td colspan="2" class="diff-lineno">Line 40:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>La Figura 3 muestra la dependencia de ''-ΔH'' (expresadas en J/g LY) '' ''con la estequiometría para todos los sistemas estudiados.</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>La Figura 3 muestra la dependencia de ''-ΔH'' (expresadas en J/g LY) '' ''con la estequiometría para todos los sistemas estudiados.</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div> </div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>[[<ins class="diffchange diffchange-inline">File</ins>:Toribio_et_al_2019a-image7-c.png|<ins class="diffchange diffchange-inline">centre|600x600px</ins>]]</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>[[<del class="diffchange diffchange-inline">Image</del>:Toribio_et_al_2019a-image7-c.png|<del class="diffchange diffchange-inline">600px</del>]]</div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div></div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td></tr>
<tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l117" >Line 117:</td>
<td colspan="2" class="diff-lineno">Line 54:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>Por otro lado, los valores de las ''T<sub>g</sub>''s son más bajos para los nanocompuestos que para el termoestable epoxídico puro, lo que estaría de acuerdo con redes más imperfectas en el caso de los nanocompuestos. Los nanocompuestos con el 6% de GNP tanto funcionalizado como sin funcionalizar, presentan variaciones muy similares de la ''T<sub>g</sub>'' con la estequiometría. Los nanocompuestos con mayor contenido de GNP<sub>NH2</sub> (10%) presentan los menores valores de ''T<sub>g</sub>'', lo que refleja la formación de redes más imperfectas, cuando son obtenidas en curados dinámicos (50-300ºC a 10ºC/min).</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>Por otro lado, los valores de las ''T<sub>g</sub>''s son más bajos para los nanocompuestos que para el termoestable epoxídico puro, lo que estaría de acuerdo con redes más imperfectas en el caso de los nanocompuestos. Los nanocompuestos con el 6% de GNP tanto funcionalizado como sin funcionalizar, presentan variaciones muy similares de la ''T<sub>g</sub>'' con la estequiometría. Los nanocompuestos con mayor contenido de GNP<sub>NH2</sub> (10%) presentan los menores valores de ''T<sub>g</sub>'', lo que refleja la formación de redes más imperfectas, cuando son obtenidas en curados dinámicos (50-300ºC a 10ºC/min).</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div> </div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>[[<ins class="diffchange diffchange-inline">File</ins>:Toribio_et_al_2019a-image8-c.png|<ins class="diffchange diffchange-inline">centre|600x600px</ins>]]</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div>[[<del class="diffchange diffchange-inline">Image</del>:Toribio_et_al_2019a-image8-c.png|<del class="diffchange diffchange-inline">600px</del>]]</div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div></div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td></tr>
<tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l125" >Line 125:</td>
<td colspan="2" class="diff-lineno">Line 61:</td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>Para analizar el efecto de los protocolos de curado (curados dinámicos en el DSC y curados isotermos en horno) en los nanocompuestos y en el termoestable puro con diferentes relaciones estequiométricas, se han comparado las temperaturas de transición vítrea de las muestras curadas de acuerdo a los dos protocolos'''.''' En la Figura 5''' '''se representan las ''T<sub>g  </sub>''de LY-XB y de  los nanocompuestos LY-XB-6%GNP<sub>NH2</sub>.</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>Para analizar el efecto de los protocolos de curado (curados dinámicos en el DSC y curados isotermos en horno) en los nanocompuestos y en el termoestable puro con diferentes relaciones estequiométricas, se han comparado las temperaturas de transición vítrea de las muestras curadas de acuerdo a los dos protocolos'''.''' En la Figura 5''' '''se representan las ''T<sub>g  </sub>''de LY-XB y de  los nanocompuestos LY-XB-6%GNP<sub>NH2</sub>.</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;"></div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div><div class="center" style="width: auto; margin-left: auto; margin-right: auto;">[[<ins class="diffchange diffchange-inline">File</ins>:Toribio_et_al_2019a-image9-c.png|<ins class="diffchange diffchange-inline">centre|600x600px</ins>]]<span style="text-align: center; font-size: 75%;">'''Figura 5.''' Variación de la  ''T<sub>g</sub>  ''con la composición XB/LY  para el termoestable  LY-XB y  los nanocompuestos LY-XB-6%GNP<sub>NH2</sub> curados en el DSC y en horno<ins class="diffchange diffchange-inline">.</ins></span></div></div></td></tr>
<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del class="diffchange diffchange-inline"> </del>[[<del class="diffchange diffchange-inline">Image</del>:Toribio_et_al_2019a-image9-c.png|<del class="diffchange diffchange-inline">600px</del>]] <span style="text-align: center; font-size: 75%;">'''Figura 5.''' Variación de la  ''T<sub>g</sub>  ''con la composición XB/LY  para el termoestable  LY-XB y  los nanocompuestos LY-XB-6%GNP<sub>NH2</sub> curados en el DSC y en horno</span></div></div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div></div></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"></td></tr>
<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>Se observa que mientras que las muestras curadas en el DSC presentan  un máximo para relaciones XB/LY=23/100 (''r'' = 1) las muestras curadas en horno alcanzan valores máximos de ''T<sub>g</sub>'' a XB/LY=25/100 y 28/100. La mayor diferencia entre las ''T<sub>g</sub>s ''de muestras curadas en horno y en DSC se encuentra cuando hay exceso de amina (''r ''> 1).</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>Se observa que mientras que las muestras curadas en el DSC presentan  un máximo para relaciones XB/LY=23/100 (''r'' = 1) las muestras curadas en horno alcanzan valores máximos de ''T<sub>g</sub>'' a XB/LY=25/100 y 28/100. La mayor diferencia entre las ''T<sub>g</sub>s ''de muestras curadas en horno y en DSC se encuentra cuando hay exceso de amina (''r ''> 1).</div></td></tr>
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Materiales.Compuestos
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Scipediacontent at 10:53, 7 May 2022
2022-05-07T10:53:30Z
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<td colspan='2' style="background-color: white; color:black; text-align: center;">Revision as of 10:53, 7 May 2022</td>
</tr><tr><td colspan="2" class="diff-lineno" id="mw-diff-left-l164" >Line 164:</td>
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<tr><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>[4] M.A. García del Cid, M.G. Prolongo, C. Salom, C. Arribas, M. Sánchez-Cabezudo, R. M. Masegosa., J. Thermal Analysis and Calorimetry '''108''', pág. 741-749 (2012).</div></td><td class='diff-marker'> </td><td style="background-color: #f9f9f9; color: #333333; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #e6e6e6; vertical-align: top; white-space: pre-wrap;"><div>[4] M.A. García del Cid, M.G. Prolongo, C. Salom, C. Arribas, M. Sánchez-Cabezudo, R. M. Masegosa., J. Thermal Analysis and Calorimetry '''108''', pág. 741-749 (2012).</div></td></tr>
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<tr><td class='diff-marker'>−</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #ffe49c; vertical-align: top; white-space: pre-wrap;"><div><del class="diffchange diffchange-inline">===</del>[5] G.R. Palmese, R.L. McCullough. J. Applied Polymer Science 46, pág.1863-73 (1992)<del class="diffchange diffchange-inline">===</del></div></td><td class='diff-marker'>+</td><td style="color:black; font-size: 88%; border-style: solid; border-width: 1px 1px 1px 4px; border-radius: 0.33em; border-color: #a3d3ff; vertical-align: top; white-space: pre-wrap;"><div>[5] G.R. Palmese, R.L. McCullough. J. Applied Polymer Science 46, pág.1863-73 (1992)</div></td></tr>
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Scipediacontent at 10:41, 7 May 2022
2022-05-07T10:41:44Z
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Scipediacontent: Scipediacontent moved page Draft Content 247086624 to Toribio et al 2019a
2022-03-31T18:51:19Z
<p>Scipediacontent moved page <a href="/public/Draft_Content_247086624" class="mw-redirect" title="Draft Content 247086624">Draft Content 247086624</a> to <a href="/public/Toribio_et_al_2019a" title="Toribio et al 2019a">Toribio et al 2019a</a></p>
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Scipediacontent: Created page with "== Abstract == In the present work the influence of the graphene type (GNP) and the different crosslinking agent ratios in the curing of graphene-epoxy dispersions and in the..."
2022-03-31T18:51:17Z
<p>Created page with "== Abstract == In the present work the influence of the graphene type (GNP) and the different crosslinking agent ratios in the curing of graphene-epoxy dispersions and in the..."</p>
<p><b>New page</b></p><div>== Abstract ==<br />
<br />
In the present work the influence of the graphene type (GNP) and the different crosslinking agent ratios in the curing of graphene-epoxy dispersions and in the glass transition temperature (Tg) of the formed nanocomposite is studied. The epoxy resin type DGEBA (LY) has been crosslinked with an aromatic polyamine (XB). Two types of graphene have been used: one non-functionalized (GNPn) and another functionalized with amino groups &nbsp;(GNPNH2). In the two systems, 5 compositions with different XB / LY ratios have been studied and, the content of graphene has been varied (6 and 10% by weight). The curing reaction has been studied by Differential Scanning Calorimetry. It has been observed that the presence of graphene accelerates the curing reaction and that the enthalpy of reaction depends on stoichiometry and graphene content. It has also been found that the variation of the Tg of the material with the stoichiometry, depends on the curing protocol.<br />
<br />
== Full document ==<br />
<pdf>Media:Draft_Content_247086624native-articles-212.pdf</pdf></div>
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